picoSpin 45/80 MHz

The picoSpin systems come with a 45 or 80 MHz proton (1H) NMR spectrometer. Liquid samples are simply injected into an internal capillary via front-panel fittings. Only 30 microliters of sample fluid is needed to obtain a spectrum. A highly stable, temperature-controlled permanent magnet to ensure easy maintenance-free operation without the need for liquid cryogens.

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Availability: Commercially Available

King Chambers
Sales Representative
king.chambers@thermofisher.com
+1 501 765 2985
46 Jonspin Road
Wilmington, MA 01887
USA
+1 978 642 1132
www.thermoscientific.com
Manufacturer
Thermo Fisher Scientific, Inc.
Product Name
picoSpin 45/80 MHz
Detection Category
Chemical;
Detection Principle
Molecular Spectroscopy;
Detection Method
Nuclear Magnetic Resonance ;
Application
Laboratory Analysis;
Product Model Number
912A0813 / 912A0813
Equipment Type
Instrument
Product Synopsis
The picoSpin systems come with a 45 or 80 MHz proton (1H) NMR spectrometer. Liquid samples are simply injected into an internal capillary via front-panel fittings. Only 30 microliters of sample fluid is needed to obtain a spectrum. A highly stable, temperature-controlled permanent magnet to ensure easy maintenance-free operation without the need for liquid cryogens.
Availability
Commercially Available
Technology Readiness Level (TRL)
9
Market Entry Date
2011
User Feedback Sources
MRIGlobal hands-on experience
Supporting Documentation
Docs: Thermo - picoSpin series II (45&80 MHz).pdf; MRIGlobal - picoSpin.pdf;
Dimensions
8 x 5.75 x 11.5 in (20.4 x 14.5 x 29.3 cm) (45 MHz) 14.3 x 10 x 17 in (36.4 x 25.4 x 43.2 cm) (80 MHz)
Weight
10.5 lbs (4.5 kg) (45 MHz), 43 lbs (19.5 kg) (80 MHz)
Power Requirements
115/230 VAC, 50/60 Hz, 150 W, no battery operation
Transportability
Person-Portable
Durability
Due to the tuned components of the internal sample probe dropping equipment is not recommended.
Operating Conditions
Indoor use only
Consumables
Solvents Syringes, Capillary cartridges custom from Thermo
Solvents/Reagents
Deuterated solvents
Calibration Schedule
Application dependent
Suggested Routine Maintenance
User may need to shim magnet and occasionally clean out capillary tube
Data Analysis Support Equipment
Needs external computer, Metrelab Mnova™ NMR software
Communications Interface
USB
Expected Operational Life
Indefinite
Shelf Life
Indefinite
Unit Cost
$31,245.00
Tested For Chemical Agents
Chemical agents that have protons (1H) can be detected
Tested For ITF-25 TIC/TIMs
TIC/TIM that have protons (1H) can be detected
Tested For Explosives
Explosives (nitroaromatics, organic peroxides) that have protons (1H) can be detected
Tested For Narcotics
Narcotics that have protons (1H) can be detected
Other Chemical Targets
Chemicals that have protons (1H) can be detected
Sample Introduction
Liquid; Solid
Sensitivity/Detection Limits
ppm; ppb
Known Interferents/Inhibitors
Mixtures containing molecules each with protons will lead to spectra that will need some expert interpretation
Start Up Time (From Cold Start To Sample Ready)
< 1 hour
Response Time (Sample Application To Output)
1 minute to hours
Total Run Time
1 minute to hours
Software Control
Laptop
Other Operational Parameters
Larmor Frequency 82 +/- 1 MHz Proton, 45 +/- 1 MHz Proton, Chemical Shift Resolution < 20 ppb FWHM (80 MHz), < 40 ppb FWHM (45 MHz)
Operator Skills Required
Technical Background
Training Available
Yes
Manuals Available
Yes
Reachback Service
No
Warranties
5 year
ITAR Export Regulations
None
IATA Shipping Restrictions
None
Data File Type Format
JCAMP DX
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